P10A.7406
Course Information
Course Semester Plan
Course Information
| No | Module Name | Development of Analytical Method Practice |
| 1 | Code of Subjects | P10A.7406 |
| 2 | Study load | 1(0-1) credits |
| 3 | Semester | 7 |
| 4 | Precondition | P10A.6408 |
| 5 | Competence | After completing this course, students are expected to applies the development of analytical methods which include standardization of analytical methods (external standards, internal standards, standard addition), optimization of analytical methods, validation of analytical methods and development of analytical methods using HPLC, and spectrophotometry. The material provided includes standardization of analysis methods with external standard techniques, internal standards, and additions; system suitability; validation of analytical methods (linearity, LOD, LOQ, precision, and accuracy); HPLC method development; and the development of spectrophotometric methods |
| 6 | Elements of Competency | MKB |
| 7 | Type Competency | Main competence |
| 8 | Syllabus | This practicum applies the development of analytical methods which include standardization of analytical methods (external standards, internal standards, standard addition), optimization of analytical methods, validation of analytical methods and development of analytical methods using HPLC, and spectrophotometry. The material provided includes standardization of analysis methods with external standard techniques, internal standards, and additions; system suitability; validation of analytical methods (linearity, LOD, LOQ, precision, and accuracy); HPLC method development; and the development of spectrophotometric methods |
| 9 | Attribute Soft Skill | Ethics, awareness, and discipline |
| 10 | Learning methods | Lab. practice, presentation, lecturer, discussion, project |
| 11 | Learning Media | Lab. equipment and LCD Projector |
| 12 | Appraisal | Task (20%); Mid Exam (40%); Final Exam (40%) |
| 13 | Lecturer | Mutakin, Ph.D., Dr. Ida Musfiroh, M.Si., Apt., and Dr. Aliya Nurhasanah, M.Si., Apt. |
| 14 | References | The United States Pharmacopoeia. 2020. United States Pharmacopoeia 2020 USP – 43 NF – 38 International Journal of Pharmaceutical Innovations, Validation of Analytical Procedure : Methodology, Review article, ISSN 2249-1031, volume 1 (2), 2011 World Health Organization, Guidelines on validation, Appendix 4 Analytical method validation, 2016 Edla, S dan B.S. Sundhar, 2014. New Analytical Method Development And Validation For The Simultaneous Estimation Of Metformin And Glibenclamide In Bulk And Tablet Dosage Form Using RP-HPLC. Rasayan, J.Chem. Vol 7 (1) : 55-63. Birajdar, A.S. 2020. New Method Development by HPLC and Validation as per ICH Guidelines. Acta Scientific Pharmaceutical Science. Vol 4 4) 55-60 |
Course Semester Plan